DIN EN ISO 15774
Animal and vegetable fats and oils - Determination of cadmium content by direct graphite furnace atomic absorption spectrometry (ISO 15774:2017); German version EN ISO 15774:2017
Tierische und pflanzliche Fette und Öle - Bestimmung von Cadmium mit Direkt-Graphitofen-Atomabsorptionsspektrometrie (ISO 15774:2017); Deutsche Fassung EN ISO 15774:2017
Overview
This International Standard describes a method for the determination of trace amounts (micrograms per kilogram) of cadmium in all types of crude or refined edible oils and fats. The oil or fat is incinerated and atomized in a suitable graphite tube furnace with a platform connected to an atomic absorption spectrometer, previously calibrated using standard solutions of an organo-compound of cadmium. The metal content is determined from the observed absorption at a wavelength of 228,8 nm. Palladium is added as a matrix modifier in order to prevent loss of cadmium during the thermal pretreatment. The International Standard has been prepared by ISO/TC 34/SC 11 "Animal and vegetable fats and oils" (secretariat: BSI, United Kingdom) of Technical Committee ISO/TC 34 "Food products" (secretariat: AFNOR, France). CEN/TC 307 "Oilseeds, vegetable and animal fats and oils and their by-products - Sampling and test methods" (secretariat: AFNOR, France) is responsible for the European Standard. On the national level, the standard is supervised by NA 057-05-05 AA "Gemeinschaftsausschuss für die Analytik von fetten, Ölen und Fettprodukten, verwandten Stoffen und Rohstoffen " (GA Fett) of the German Society for Fat Science (DGF) ("Joint committee for the analysis of fats, oils and products thereof, related and primary products") and DIN Standards Committee Food and Agricultural Products (NAL).