NA 119

DIN Standards Committee Water Practice

Project

Environmental solid matrices - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS) (ISO/DIS 16965:2024); German and English version prEN ISO 16965:2024

Abstract

This document specifies a method for the determination of the following elements in aqua regia, nitric acid or mixture of hydrochloric (HCl), nitric (HNO3) and tetrafluoroboric (HBF4)/hydrofluoric (HF) acid digests of soil, treated biowaste, waste, sludge and sediment using inductively coupled plasma mass spectrometry (ICP-MS): Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rhenium (Re), rhodium (Rh), rubidium (Rb), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulfur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr). The working range depends on the matrix and the interferences encountered. The method detection limit of the method is between 0,1 mg/kg dry matter and 2,0 mg/kg dry matter for most elements. The limit of detection will be higher in cases where the determination is likely to be interfered or in case of memory effects

Begin

2022-05-16

WI

00444248

Planned document number

DIN EN ISO 16965

Project number

11904770

Responsible national committee

NA 119-01-02-02-04 AK - Elementary analysis  

Responsible european committee

CEN/TC 444/WG 3 - Inorganic analysis  

Responsible international committee

ISO/TC 190/SC 3/WG 1 - Inorganic analysis  

draft standard

Environmental solid matrices - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS) (ISO/DIS 16965:2024); German and English version prEN ISO 16965:2024
2024-08
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previous edition(s)

Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS); German version EN 16171:2016
2017-01

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Contact

Dr.

Anja Sokolowski

Am DIN-Platz, Burggrafenstr. 6
10787 Berlin

Tel.: +49 30 2601-2547
Fax: +49 30 2601-42547

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