DIN Standards Committee Food and Agricultural Products
DIN EN 15550
Animal feeding stuffs - Methods of sampling and analysis - Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion; German version EN 15550:2017
Futtermittel - Probenahme- und Untersuchungsverfahren - Bestimmung von Cadmium und Blei mittels Graphitrohrofen-Atomabsorptionsspektrometrie (GF-AAS) nach Druckaufschluss; Deutsche Fassung EN 15550:2017
Overview
DIN EN 15550 specifies a method for the determination of the elements cadmium and lead in animal feeding stuffs by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion. The method was successfully tested in the range of 0,015 mg/kg to 5,65 mg/kg for Cd and 0,18 mg/kg to 40,3 mg/kg for lead in 11 animal feeds: 2 complete feeds (pig feed, sheep feed), 2 complementary feeds (2 mineral feeds), 1 mineral premixture, 4 feed materials (MgO, 2 phosphates, CaCO3) and 2 feed additives (CuSO4, bentonite). For the determination of extractable lead in minerals and feeds, containing phyllosilicates (such as kaolinite clay) wet digestion with diluted nitric acid should be used. The method limit of quantification for each element is dependent on the sample matrix as well as the instrument. For cadmium a limit of quantification of 0,05 mg/kg should normally be obtained while for lead, a limit of quantification of 0,5 mg/kg should be obtained. The European Standard has been prepared by Technical Committee CEN/TC 327 "Animal feeding stuffs - Methods of sampling and analysis", the secretariat of which is held by NEN (Netherlands). The responsible German standardization committee is Working Committee NA 057-03-03 AA "Futtermittel" ("Animal feeding stuffs") at DIN Standards Committee Food and Agricultural Products (NAL).
Responsible national committee
NA 057-03-03 AA - Animal feeding stuffs