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4. NAL

DIN Standards Committee Food and Agricultural Products

Overview

This standard describes a method for the determination of calcium, copper, iron, magnesium, manganese, phosphorus, potassium, sodium, sulfur and zinc in different foodstuffs using optical emission spectrometry with inductively coupled plasma (ICP-OES) after pressure digestion. This method has been validated in an interlaboratory study according to ISO 5725 on infant formula soya based, cheese, chicken meat, wheat flour, apple juice, lobster and milk. After digestion of the sample with the pressure digestion process described in EN 13805, calcium, copper, iron, magnesium, manganese, phosphorus, potassium, sodium, sulfur and zinc are determined quantitatively with the ICP-OES. The digestion solution is nebulized, the aerosol is directed into an inductively coupled argon plasma, where the elements are atomized and excited for radiation. The emission radiation is resolved spectrally and its intensity determined at element-specific wavelengths with a detector system. Ionization interference can be minimized using an ionization buffer. This document has been prepared by Technical Committee CEN/TC 275 "Food analysis - Horizontal methods", the secretariat of which is held by DIN. The responsible German committee is Working Committee NA 057-01-09 AA "Elemente und ihre Verbindungen" ("Elements and their chemical species") at the DIN Standards Committee Food and Agricultural Products (NAL).

Responsible national committee

NA 057-01-09 AA - Elements and their chemical species  

Responsible european committee

CEN/TC 275/WG 10 - Elements and their chemical species